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Beilstein J. Org. Chem. 2006, 2, No. 10, doi:10.1186/1860-5397-2-10
Graphical Abstract
Figure 1: Representative self-terminating radical reactions.
Figure 2: Self-terminating, oxidative and chain mechanisms for evolution of 6 to 2.
Figure 3: Proposed β-fragmentation reactions to form acyl and alkoxycarbonyl radicals.
Scheme 1: Synthesis of fragmentation probe substrates 11a,b
Figure 4: Competing mechanistic pathways for reaction of 11 with Bu3SnH.
Scheme 2: Synthesis of authentic samples of products